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1，2-二氯乙烷以及0.1g～5g催化剂，加入三口瓶中，其中有机腈与缩甲醛的摩尔比为3.5～5∶1；在搅拌下加热至反应液回流，持续搅拌2h～20h，停止加热，反应结束。趁热过滤反应液分离出催化剂后，滤液减压除溶剂，室温静置10h～12h，过滤得1，3，5-三取代六氢均三嗪。本发明主要用于1，3，5-三取代六氢均三嗪的合成。","西安近代化学研究所","2026-10-12T00:54:35.109Z","2010.06.09#公开;2011.01.26#实质审查的生效;2012.01.04#授权","CN200910250472.1","C07D251\u002F04","吕剑;杨建明;余秦伟;刘波;李凤仙;谷玉杰",[],[],{"resultType":8,"id":306,"title":307,"abstract":308,"orgName":297,"province":13,"date":298,"trl":15,"transferMode":15,"keywords":15,"industry":15,"patentType":16,"legalStatus":309,"isOpenLicense":18,"isRevitalized":19,"techMaturity":15,"starRating":15,"licenseFeeText":15,"patentNo":310,"ipc":311,"inventors":312,"tags":313,"tagNames":314},"gpi_01884","N-硝基乙酰胺的制备方法","本发明公开一种N-硝基乙酰胺的制备方法，该方法将硝酰胺、乙酰氯加入50mL～200mL有机溶剂中，其中有机溶剂为乙腈、乙醚、乙酸乙酯中的一种，硝酰胺与乙酰氯摩尔比为1∶0.8～1.2，在反应温度20℃～40℃条件下反应6h～10h，反应液蒸除溶剂，所得固体在正己烷中重结晶，干燥后得N-硝基乙酰胺。该方法收率高，反应时间短。主要用于制备N-硝基乙酰胺。","2011.02.16#公开;2011.03.30#实质审查的生效;2013.04.03#授权","CN201010525313.0","C07C243\u002F02;C07C241\u002F00","杨建明;吕剑;李亚妮;刘波;薛云娜;谷玉杰",[],[],{"resultType":8,"id":316,"title":317,"abstract":318,"orgName":297,"province":13,"date":298,"trl":15,"transferMode":15,"keywords":15,"industry":15,"patentType":16,"legalStatus":319,"isOpenLicense":18,"isRevitalized":19,"techMaturity":15,"starRating":15,"licenseFeeText":15,"patentNo":320,"ipc":311,"inventors":321,"tags":322,"tagNames":323},"gpi_01885","N-硝基氨基乙醇的制备方法","本发明公开了一种N-硝基氨基乙醇的制备方法，该方法将环氧乙烷溶解于氯代烃中，缓慢滴加到含有硝酰胺的氯代烃中，其中氯代烃为二氯甲烷、三氯甲烷、四氯化碳中的一种，环氧乙烷与硝酰胺摩尔比为1∶0.8～1.2，在反应温度0℃～30℃条件下反应2h～6h，反应液蒸除溶剂，得N-硝基氨基乙醇，具有反应收率高的特点。","2011.02.16#公开;2011.03.30#实质审查的生效;2013.03.06#授权","CN201010525314.5","杨建明;吕剑;余秦伟;李凤仙;刘波;王伟",[],[],778,1,30,26,{"list":329,"total":341,"page":325,"pageSize":325,"totalPages":341},[330],{"id":331,"name":332,"orgName":333,"school":15,"gender":15,"title":15,"degree":15,"honor":334,"position":335,"researchDirection":336,"intro":15,"province":15,"completeness":337,"avatarAuthorized":18,"sourceUrl":338,"nameValid":19,"tags":339,"tagNames":340},"cmv7rn1er000jddmmau8qulzd","应汉杰","苏州大学","ACADEMICIAN","苏州大学校长","生物制造与酶催化方向专家",80,"chaingraph:\u002F\u002F应汉杰",[],[],35346]